本方法適用于惡臭污染源排氣和環(huán)境空氣中硫化氫、甲硫醇、甲硫醚和二甲二硫的同時測定。氣相色譜儀的火焰光度檢測器(GC-FPD)對四種成分的檢出限為0.2╳10-3~1.0╳10-3g,當氣體樣品中四種成分濃度高于1.0mg/m3時,可取1~2mL氣體樣品直接注入氣相色譜儀分析。對1L氣體樣品進行濃縮,四種成分的方法檢出限分別為.2╳10-3~1.0╳10-3mg/m3。
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浩瀚色譜(山東)應用技術開發(fā)有限公司,采用冷阱預濃縮-氣相色譜/質(zhì)譜聯(lián)用法測定環(huán)境空氣中硫化氫、甲硫醇、甲硫醚、二硫化碳、二甲二硫、噻吩等6種硫化物,討論了采樣容器材質(zhì)的影響。方法線性良好,6種硫化物的檢出限為1.3μg/m3~5.2μg/m3,混合標準氣平行測定的RSD≤8.6%
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名稱:硫化物測定專用柱
型號:HH一sulfide-III
規(guī)格:3m*3mm
zui高使用溫度:120°C
應用:GB/T 14678-1993 《空氣質(zhì)量 硫化氫、甲硫醇、甲硫醚和二甲二硫的測定 氣相色譜法》
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適用于:
安捷倫490在線/便攜,4890,5890,6890,7820,7890,8860,8890
島津GC-14C,GC-2010,GC-2014,GC-2030
賽默飛1310,1300,1610,1600
瓦里安3800系列
布魯克PE580,590,680,690
磐諾A90,福立GC9790,華愛,天瑞,天美,GC7900,川儀,北分瑞利,東西電子,魯南瑞虹,捷島/科曉
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This method is applicable for the simultaneous determination of hydrogen sulfide, methyl mercaptan, methyl sulfide, and dimethyl disulfide in the exhaust gas of odor pollution sources and ambient air. The detection limit of the flame photometric detector (GC-FPD) of the gas chromatograph for four components is 0.2-10-3 to 1.0-10-3g. When the concentration of the four components in the gas sample is higher than 1.0mg/m3, 1-2mL of gas sample can be directly injected into the gas chromatograph for analysis. Concentrate a 1L gas sample, and the detection limits for the four components are. 2 ╳ 10-3 to 1.0 ╳ 10-3mg/m3, respectively.
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. used cold trap pre concentration gas chromatography/mass spectrometry to determine six sulfides including hydrogen sulfide, methyl mercaptan, methyl sulfide, carbon disulfide, dimethyl disulfide, and thiophene in ambient air, and discussed the influence of sampling container materials. The method has good linearity, with detection limits of 1.3 μ g/m3 to 5.2 μ g/m3 for 6 sulfides, and RSD ≤ 8.6% for parallel determination of mixed standard gas
Name: Special Column for Sulfide Determination
Model: HH sulfade-III
Specification: 3m * 3mm
Maximum operating temperature: 120 ° C
Application: GB/T 14678-1993 "Air quality - Determination of hydrogen sulfide, methyl mercaptan, methyl sulfide and dimethyl disulfide - Gas chromatographic method"
Suitable for:
Agilent 490 online/portable, 48905890689088608890
Shimadzu GC-14C, GC-2010, GC-2014, GC-2030
Thermo Fisher Scientific 1310130016101600
Varian 3800 Series
Brooke PE580590680690
Panno A90, Fuli GC9790, Huaai, Tianrui, Tianmei, GC7900, Chuanyi, Beifen Ruili, Dongxi Electronics, Lunan Ruihong, Jiedao/Kexiao
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