工業(yè)氫氣分析項(xiàng)目執(zhí)行國(guó)家標(biāo)準(zhǔn)(GB/T3634.1—2006).其中氧、氬和氮含量的測(cè)定采用的是氣相色譜法,配備脫氧柱和切換柱兩次進(jìn)樣,測(cè)定樣品氣中氬和氮的含量,用差減法計(jì)算出樣品.此方法人為地兩次手動(dòng)進(jìn)樣,每次分析樣品在六通閥的定量管中由于受溫度壓力不同給分析結(jié)果帶來(lái)人為誤差.
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為解決現(xiàn)有氣相色譜法在對(duì)氧氣、氬氣、氮?dú)獾葰怏w通過(guò)色譜柱進(jìn)行分析測(cè)定時(shí)存在色譜柱老化后氧氬峰和氮?dú)夥宸蛛x度降低無(wú)法進(jìn)行氣體測(cè)定及工藝不穩(wěn)定操作下脫氧柱有效利用率低的缺陷。
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浩瀚色譜（山東）應(yīng)用技術(shù)開(kāi)發(fā)有限公司，針對(duì)國(guó)標(biāo)氫中氧氬測(cè)定的2個(gè)閥，2次進(jìn)樣，401脫氧柱壽命短等的不足，研制1根專用填充柱測(cè)定氧氬，分析時(shí)間短，3分鐘完成一次分析，氧氬分離度大，峰型對(duì)稱，效率高。
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名稱：HH-O2AR填充柱
規(guī)格：3m*1/8，60-80Mesh
使用溫度：180°C
應(yīng)用：工業(yè)氫中氧氬測(cè)定的1柱1次進(jìn)樣系統(tǒng)
適用于：
安捷倫490在線/便攜，4890,5890,6890,7820,7890,8860,8890
島津GC-14C，GC-2010，GC-2014，GC-2030
賽默飛1310,1300,1610,1600
瓦里安3800系列
布魯克PE580,590,680,690
磐諾A90，福立GC9790，華愛(ài)，天瑞，天美，GC7900，川儀，北分瑞利，東西電子，魯南瑞虹，捷島/科曉
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The industrial hydrogen analysis project follows the national standard (GB/T3634.1-2006). The determination of oxygen, argon, and nitrogen content is carried out using gas chromatography, equipped with a deoxygenation column and a switching column for two injections. The content of argon and nitrogen in the sample gas is determined, and the sample is calculated by subtraction This party has manually injected samples twice, and each time the sample is analyzed in the quantitative tube of the six way valve, the analysis results are subject to human error due to temperature and pressure differences
To address the shortcomings of existing gas chromatography methods in analyzing and determining gases such as oxygen, argon, and nitrogen through chromatographic columns, such as decreased separation of oxygen argon and nitrogen peaks due to column aging, inability to perform gas determination, and low effective utilization of deoxygenation columns under unstable process operation.
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed a dedicated packed column for the determination of oxygen and argon in hydrogen, addressing the shortcomings of the national standard, such as two valves, two injections, and short lifespan of the 401 deoxygenation column. The analysis time is short, with one analysis completed in 3 minutes. The oxygen and argon separation is high, the peak shape is symmetrical, and the efficiency is high.
Name: HH-O2AR Filled Column
Specification: 3m * 1/8, 60-80 Mesh
Operating temperature: 180 ° C
Application: One column, one injection system for the determination of oxygen and argon in industrial hydrogen
Applicable to:
Agilent 490 online/portable, 48905890689088608890
Shimadzu GC-14C, GC-2010，GC-2014，GC-2030
Thermo Fisher Scientific 1310130016101600
Varian 3800 Series
Brooke PE580590680690
Panno A90, Fuli GC9790, Huaai, Tianrui, Tianmei, GC7900， Chuanyi, Beifen Ruili, Dongxi Electronics, Lunan Ruihong, Jiedao/Kexiao
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