GB/T 43571-2023
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本文件描述了玩具材料中11種可遷移有機(jī)錫測定的氣相色譜-串聯(lián)質(zhì)譜法.本文件適用于玩具材料中甲基錫(MeT),二甲基錫(DMT),二丙基錫(DProT),丁基錫(BuT),二丁基錫(DBT),三丁基錫(TBT),正辛基錫(MOT),二辛基錫(DOT),四丁基錫(TeBT),二苯基錫(DPhT),三苯基錫(TPhT)11種可遷移有機(jī)錫的測定.
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名稱：安捷倫GC8860玻璃柱
規(guī)格：6ft*1/4
型號：10%DC550/Chromosorb WAW DMCS 60-80目
zui高使用溫度：240°C
應(yīng)用：單丁基三氯化錫，二丁基二氯化錫
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浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司，研制生產(chǎn)的《DC-550玻璃色譜柱應(yīng)用安捷倫8890TCD》，提出了以乙基溴化鎂作為衍生化試劑 ,將二丁基二氯化錫轉(zhuǎn)化成低沸點、易汽化的二丁基二乙基錫 ,采用四丁基錫作內(nèi)標(biāo) ,測定二丁基二氯化錫含量的氣相色譜法。方法具有分析速度快、準(zhǔn)確度高、重現(xiàn)性好等優(yōu)點。此方法回收率為 97.5 % -1 0 0.9% 。
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適用于：
安捷倫490在線/便攜，4890,5890,6890,7820,7890,8860,8890
島津GC-14C，GC-2010，GC-2014，GC-2030
賽默飛1310,1300,1610,1600
瓦里安3800系列
布魯克PE580,590,680,690
磐諾A90，福立GC9790，華愛，天瑞，天美，GC7900，川儀，北分瑞利，東西電子，魯南瑞虹，捷島/科曉
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GB/T 43571-2023
This document describes the gas chromatography tandem mass spectrometry method for the determination of 11 transferable organotin compounds in toy materials This document is applicable for the determination of 11 migratory organotin compounds in toy materials, including methyl tin (MeT), dimethyl tin (DMT), dipropyltin (DProT), butyl tin (BuT), dibutyltin (DBT), tributyltin (TBT), octyltin (MOT), dioctyltin (DOT), tetrabutyltin (TeBT), diphenyltin (DPhT), and triphenyltin (TPhT)
Name: Agilent GC8860 Glass Column
Specification: 6ft * 1/4
Model: 10% DC550/Chromosorb WAW DMCS 60-80 mesh
Maximum operating temperature: 240 ° C
Application: Monobutyl tin trichloride, dibutyl tin dichloride
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed and produced the "DC-550 Glass Chromatography Column Application Agilent 8890TCD", which proposes using ethyl magnesium bromide as a derivatization reagent to convert dibutyltin dichloride into low boiling point, easily vaporized dibutyltin, and using tetrabutyltin as an internal standard to determine the content of dibutyltin dichloride by gas chromatography. The method has the advantages of fast analysis speed, high accuracy, and good reproducibility. The recovery rate of this method is 97.5% -100.9%.
Suitable for:
Agilent 490 online/portable, 48905890689088608890
Shimadzu GC-14C, GC-2010, GC-2014, GC-2030
Thermo Fisher Scientific 1310130016101600
Varian 3800 Series
Brooke PE580590680690
Panno A90, Fuli GC9790, Huaai, Tianrui, Tianmei, GC7900， Chuanyi, Beifen Ruili, Dongxi Electronics, Lunan Ruihong, Jiedao/Kexiao
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